D-amino acid series ji bo synthesiya Solid Phase
Kîtekîteya Hilbera
| No | Wer | Cas No. | Nîşana kalîteya key | ||||
| Qiralîtî | Isomer | Nepenîtiya taybetî | * Max1 | Şilî | |||
| 1 | FMOC-D-ALA-OH.H2O | 799990-15-1 | 999.5% | ≤0.1% | ≤0.1% | ≤ %,2% | ≤6.5% |
| 2 | FMOC-3- (2-naphthyl) -d-ala-oh | 138774-94-4 | ≥99.0% | ≤ %,2% | ≤2.3% | ≤2.3% | ≤1.0% |
| 3 | AC-3- (2-Naphthyl) -D-Ala-Oh | 37440-01-0 | ≥99.0% | ≤ %,2% | ≤2.3% | ≤2.3% | ≤1.0% |
| 4 | Fmoc-3- (3-Pyridinyl) -d-ala-oh | 142994-45-4 | ≥99.0% | ≤ %,2% | ≤2.3% | ≤2.3% | ≤1.0% |
| 5 | FMOC-D-APH (tBUCBM) -OH | 1433975-21-3 | ≥99.0% | ≤ %,2% | ≤2.3% | ≤2.3% | ≤1.0% |
| 6 | Fmoc-D-Aph (CBM) -OH | 324017-22-3 | ≥99.0% | ≤ %,2% | ≤2.3% | ≤2.3% | ≤1.0% |
| 7 | Fmoc-D-Aph (hor) -oh | NA | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 8 | Fmoc-Aph (D-hor) -oh | NA | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 9 | Fmoc-D-Arg (PBF) -OH | 187618-60-6 | ≥99.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤2.0% |
| 10 | FMOC-D-ARG (NO2) -OH | 160347-94-4 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤2.0% |
| 11 | Fmoc-D-Homoarg (PBF) -OH | 401915-53-5 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤2.0% |
| 12 | Fmoc-D-Homoarg (ET) 2-Oh | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤2.0% |
| 13 | FMOC-D-ASN (TRT) -OH | 180570-71-2 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 14 | FMOC-D-ASP (Otbu) -OH | 112883-39-3 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 15 | Fmoc-D-ASP-OTBU | 34098-70-7 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 16 | FMOC-D-ASP (Oall) -OH | 177609-12-0 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 17 | Fmoc-D-Cit-Oh | 2003444-33-8 | 999.5% | ≤0.1% | ≤0.1% | ≤ %,2% | ≤1.0% |
| 18 | FMOC-D-CY (TRT) -OH | 167015-11-4 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 19 | Fmoc-D-Cys (ACM) -OH | 168300-88-7 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 20 | Fmoc-D-Cys (MMT) -OH | 1198791-73-9 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 21 | FMOC-D-GLN (TRT) -OH | 200623-62-7 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤2.0% |
| 22 | FMOC-D-GLU (OTBU) -oh.h2o | 104091-08-9 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤5.0% |
| 23 | Fmoc-D-glu-Otbu | 109745-15-5 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 24 | Hd-glu-otbu | 25456-76-2 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 25 | Fmoc-D-wî (TRT) -OH | 135610-90-1 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 26 | Boc-d-wî (TRT) -OH | 393568-74-6 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 27 | Fmoc-D-wî (BZL) -oh | 1417638-37-9 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 28 | Fmoc-D-Ile-OH | 143688-83-9 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 29 | Fmoc-D-Allo-ile-OH | 118904-37-3 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 30 | Fmoc-D-Leu-OH | 114360-54-2 | 999.5% | ≤0.1% | ≤0.1% | ≤ %,2% | ≤1.0% |
| 31 | FMOC-D-Lys (BOC) -OH | 92122-45-7 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 32 | Fmoc-D-Lys (Dabeş) -OH | 214750-75-1 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 33 | Fmoc-D-Lys (ivdde) -oh | 1272755-33-5 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 34 | Fmoc-D-Lys (MMT) -OH | 198544-94-4 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 35 | FMOC-D-Lys (IPR, BOC) -OH | NA | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 36 | Fmoc-D-Lys (Nicotinoyl) -OH | 252049-12-0 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 37 | Fmoc-D-Met-Oh | 112883-40-6 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 38 | Fmoc-D-Orn (BOC) -OH | 118476-89-4 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 39 | Fmoc-D-Phe-Oh | 86123-10-6 | 999.5% | ≤0.1% | ≤0.1% | ≤ %,2% | ≤1.0% |
| 40 | Fmoc-4-Chloro-D-Phe-Oh | 142994-19-2 | ≥99.0% | ≤ %,2% | ≤2.3% | ≤2.3% | ≤1.0% |
| 41 | FMOC-D-PRO-OH.H2O | 101555-62-8 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤6.0% |
| 42 | D-Pyr-Oh | 4042-36-8 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 43 | Fmoc-D-Ser (TBU) -OH | 128107-47-1 | 999.5% | ≤0.1% | ≤0.1% | ≤ %,2% | ≤1.0% |
| 44 | Fmoc-D-Ser (TRT) -OH | 212688-51-2 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 45 | FMOC-D-thR (TBU) -OH | 138797-71-4 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 46 | FMOC-D-TRP (BOC) -OH | 163619-04-3 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤2.0% |
| 47 | Fmoc-2-Methyl-D-Trp-Oh | 196808-79-4 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤2.0% |
| 48 | Fmoc-D-Tyr (TBU) -OH | 118488-18-9 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 49 | Fmoc-D-Tyr (ET) -OH | 162502-65-0 | 999.5% | ≤0.1% | ≤0.1% | ≤ %,2% | ≤1.0% |
| 50 | Fmoc-D-Tyr (Me) -OH | 201335-88-8 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 51 | FMOC-N-ME-D-TYR (TBU) -OH | 196808-79-4 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 52 | Fmoc-D-Tyr (BZL) -oh | 138775-48-1 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 53 | Fmoc-D-Val-Oh | 84624-17-9 | ≥98.5% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 54 | Fmoc-D-Hyp (TBU) -OH | 464193-92-8 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 55 | Fmoc-D-Thi-Oh | 201532-42-5 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 56 | Fmoc-D-Tic-Oh | 130309-33-0 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 57 | Fmoc-D-Oic-Oh | 130309-37-4 | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 58 | Boc-D-wî (TRT) -Aib-Oh | NA | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 59 | FMOC-D-GLU (OTBU) -gly-oh | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 60 | Boc-D-wî (TRT) -Aib-Glu (Otbu) -gly-Oh | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 61 | Boc-wî (TRT) -Aib-D-Glu (Otbu) -gly-Oh | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 62 | Boc-D-wî (TRT) -Aib-D-Glu (Otbu) -gly-oh | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 63 | Fmoc-D-Arg (PBF) -gly-Oh | NA | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 64 | Fmoc-D-Ala-Ala-OH | NA | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 65 | Fmoc-Ala-D-Ala-Oh | NA | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 66 | Fmoc-D-Ala-D-Ala-Oh | NA | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 67 | Fmoc-D-Lys (Palm-Glu-Otbu) -OH | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 68 | Fmoc-lys (palm-d-glu-otbu) -oh | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 69 | Fmoc-D-Lys (Palm-D-Glu-Otbu) -OH | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
| 70 | Octa (Otbu) -d-glu-otbu | NA | ≥98.0% | ≤ %,2% | ≤2.3% | ≤0.5% | ≤1.0% |
| 71 | Octa (Otbu) -d-glu (ɑ-otbu) -Aeea-aeea-oh | NA | ≥95.0% | ≤0.5% | ≤1.0% | ≤2.0% | ≤1.0% |
* Max1 = Paqijiya naskirî ya Max
Agahiyên din:
- acîdê acetîk: ≤0.02% (hemî hilber)
- Ethyl Acetate: ≤0.5% (hemî hilber)
- alkol: ≤0.5% (hemî hilber)
Ava paqij
Ava paqijkirî di hilberîn û amûrên paqijkirina API-ê de tête bikar anîn. Avê paqijkirî ji hêla ava bajêr ve tête çêkirin, bi navgîniya dermankirinê (filterê pir-medya, nermalava karbonê, hwd.) Av bi berdewamî di 25 ± 2 ℃ de bi rêjeya leza 1.2m / s diherike.
